第 31 卷第 5 期 Vol. 31 No. 5 2001 年 10 月 Oct 2001

所属栏目：分析与测试 1-(2-氯苯基)-5(4H)-四唑啉酮气相色谱法的分析研究

潘忠稳; 姚琼; 凌冰(安徽省化工研究院)

摘　要：用 5 %OV - 17,长度为 2m的玻璃填充柱 ,以硝基苯为内标物 ,在 140℃柱温下 ,用FID检测器对 1 (2 氯苯基 ) 5 (4H ) 四唑啉酮进行定量分析。该方法变异系数为0 2 2 % ,平均回收率 99 8% ,线性相关系数为 0 99998

关键词：气相色谱法; 1（2氯苯基）5（4H）四唑啉酮; 分析

中图分类号：TQ252.8　　文献标识码：A　　文章编号：1009-9212(2001)05-0047-02

Analysis of 1-(2-Chlorophenyl)-5(4H)-tetrazolinone by Gas Chomatography

PAN Zhong wen; YAO Qiong; LING Bing （Anhui Research Institute of Chemical Industry; Hefei 230041）

Abstract：chlorophenyl) 5(4H) tetrazolinone was analyzed by gas chomatography with flame ionization detection on Φ2.5mm×2m 5% OV-17/Gas chromosorb W HP (0.147～0.175mm) packed column. The column temperature was 140℃. The ionization temperature was 240℃ and the detection temperature was 240℃. The linear relationship of this method was very good. The standard deviated and viation coefficient were 0.21% and 0.22% respectively.

Key words：chlorophenyl） 5（4H） tetrazolinone; analysis; gas chomatography

收稿日期：2001-08-12

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