第 32 卷第 1 期 | | Vol. 32 No. 1 | 2002 年 2 月 | Feb 2002 |
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所属栏目:其它
2-甲氧基丙烯的制备研究 |
杨淑敏; 王海民; 刘鸿(西安近代化学研究所; 陕西西安) |
摘 要:2 ,2 二甲氧基丙烷在 115℃发生消去反应可得 2 甲氧基丙烯 ,精馏收率 80 6% ,纯度大于 98% ,用红外及核磁光谱验证了产品结构 |
关键词:2甲氧基丙烯; 2; 2二甲氧基丙烷; 制备 |
中图分类号:TQ223.2 文献标识码:A 文章编号:1009-9212(2002)01-0020-02 |
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Synthesis of 2-methoxypropene. |
YANG Shu min; et al.(Xi'an Modern Chemistry Research Insitute; Xi'an 710065) |
Abstract:Methoxypropene was obtained by the elimination of methanol from 2,2 dimethoxypropane at 115℃ gave the final compound.The distillation was 80.6% with the purity of 98%.The structure was confirmed by IR and 1HNMR. |
Key words:methoxypropene; 2 2methoxypropane; preparation |
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收稿日期:2001-08-10
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