| 第 32 卷第 2 期 |  | Vol. 32 No. 2 | | 2002 年 4 月 | Apr 2002 |
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所属栏目：分析与测试
三相萃取分离法测定铅丹中痕量杂质元素 |
| 刘立平; 易晓明(湖南省地质工程勘察院; 湖南省矿产测试利用研究所; 湖南株洲; 湖南长沙) |
| 摘 要：研究了三相萃取分离法测定铅丹 (四氧化三铅 )中Fe、Cu、Ni、Co、Mn、Zn、Cd等痕量杂质元素的分析方法 ,考察了Pb基体对待测元素的干扰情况。方法检出限 0 0 6～ 0 6 μg/g ,加标回收率均 >87% ,标准回收变动系数 <10 % |
| 关键词：三相萃取; 杂质元素; 四氧化三铅 |
| 中图分类号：TQ134.3+3 文献标识码：A 文章编号：1009-9212(2002)02-0060-02 |
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| Determination of trace impure elements In Red Lead by ICP-AES after Separsted from tri-phase extraction. |
| Liu Li ping 1; Yi Xiao ming 2.（1.Hunan Institute of Geology and Engineering Survey; Zhuzhou 412003; China; 2.Hunan Institute of Mineral Resources Testing and Utilization; Changsha 410007; China） |
| Abstract：A sensitive analytical method of trace impure elements in red lead (Pb 3O 4) by ICP AES after separated from tri phase extraction has been studied, such as Fe?Cu?Ni?Co?Mn?Zn?Cd etc. The dioturbances of determined elements from lead matrix are inspected. The detection limits of the method is 0.06～0.6μg/g. The rates of standard additions recovery are all higher than 87%, RSD are varied within 10%. |
| Key words：tri phase extraction; impure elements; Pb 3O 4 |
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收稿日期：2001-09-18
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