| 第 32 卷第 2 期 |  | Vol. 32 No. 2 | | 2002 年 4 月 | Apr 2002 |
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所属栏目：其它
纳米氧化锌的制备与表征 |
| 刘敏娜; 王桂清; 罗成; 徐英(湘潭大学化学学院; 兰州化学物理研究所; 湖南湘潭; 甘肃兰州) |
| 摘 要：对传统的直接沉淀法进行了改进 ,对反应温度、搅拌速度、投料方式及洗涤条件等多种因素对产物纳米氧化锌的影响进行了研究。结果表明 ,改进的直接沉淀法制备纳米氧化锌具有工艺简单、成本较低 ,能够得到六方晶系、球形 ,粒径约为 15～ 2 5nm的纳米氧化锌 |
| 关键词：纳米氧化锌; 直接沉淀法; 合成; 表征 |
| 中图分类号：TQ132.4 文献标识码：A 文章编号：1009-9212(2002)02-0034-03 |
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| Synthesis and Characterization of Nanometer-sized Zine Oxide. |
| Liu Min na; et al（Deparment of Chemistry Xiangtan University; Xiangtan 411105; China） |
| Abstract：Nanometer sized ZnO was synthesized by direct precipitation. The effects of reaction temperature, stirring, charging up and washing condition of product were studied. And the best reaction condition was comfirmed by orthogonal experiments.The research indicated that modified direct precipitation was superior to commercial homogeneous precipitation, with simple methodology and low cost. The ZnO particles prepared are spherical, hexagonal structure, and their demension are small. |
| Key words：nanometer sized ZnO; direct precipitation; synthesis; characterization |
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收稿日期：2002-02-23
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