| 第 32 卷第 3 期 |  | Vol. 32 No. 3 | | 2002 年 6 月 | Jun 2002 |
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所属栏目：分析与测试
用双道原子荧光计同时测定化探样品中的砷和锑 |
| 郭腊梅; 易晓明(矿产测试利用研究所; 湖南长沙41007) |
| 摘 要：采用AFS 12 0 1型双道原子荧光光度计对化探样品的砷和锑进行同时测定试验。用硝酸铵 -硫酸铵混合铵盐消化样品在盐酸溶液中与 2 %硼氢化钾生成砷化氢和锑化氢气体 ,其气体导入原子化石英燃烧炉进行原子化 ,砷和锑的热原子蒸气吸收特定波长的激发光之后发荧光 ,其荧光强度与砷、锑含量成正比 ,通过测定样品和标准的荧光强度 ,AFS 12 0 1型双道原子荧光光工计自动计算打印出分析结果。 |
| 关键词：AFS-1201型双原子荧光计; 化探样品; 铵盐熔样; 砷; 锑 |
| 中图分类号：TQ126.4 文献标识码：A 文章编号：1009-9212(2002)03-0041-02 |
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| The meanwhile analysis of As and Sb in the geochemical exploration sample by double-channel atomic fluorophotometer. |
| Guo La-mei; et al（Hunan Institute of Mineral Resources Testing and utilization; Changsha Hunan 410007; China） |
| Abstract：The meanwhile analysis of As and Sb in the geochemical exploration sample were reported by double-channel atomic fluorophotometer of AFS-1201 type.NH 4NO 3-(NH 4) 2SO 4-and ammonium salt were used to digest the sample and grow into AsH 3 and SbH 3 gas in HCl solution with two Perlent KBH 4. The gas which is led to quartz combustion tube burner is atomized. The hot atomic steam As and Sb sends out fluo rescence after absorbing definite wavelength of exciting line.The intensity of fluorescence and the... |
| Key words：double-channel atomic fluorophotometer; geochemical exploration sample; ammonium salt solutional sample |
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收稿日期：2002-05-14
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