第 49 卷第 6 期Vol. 49 No. 6
2019 年 12 月Dec 2019

所属栏目:分析与测试

30%丙环唑·咪鲜胺水乳剂的气相色谱分析
潘光飞,祁康旭,程希希,王 炜,卢城炜,蒋成刚,徐 瑶 (浙江禾本科技股份有限公司,浙江 温州 325008)
摘 要:使用键合5%苯甲基硅酮为固定相的毛细管柱,采用气相色谱法,对试样中的丙环唑和咪鲜胺进行定量测定。结果表明,丙环唑和咪鲜胺的线性相关系数分别为0.999 9和0.999 8,标准偏差分别为0.035和0.028,变异系数分别为0.34%和0.14%,平均回收率分别为99.88%和99.95%。
关键词:丙环唑;咪鲜胺;气相色谱
中图分类号:O657.7  文献标识码:A  文章编号:1009-9212(2019)06-0070-03
Analysis Method for 30% EW of Propiconazole and Prochloraz by GC
PAN Guang-fei , QI Kang-xu, CHEN Xi-xi, WANG Wei, LU Chen-wei, JIANG Cheng-gang, XU Yao (Zhejiang Heben Pesticide & Chemicals Co., Ltd., Wenzhou 325008, China)
Abstract:The quantitative determination of propiconazole and prochloraz in samples was carried out by gas chromatography equipped with a capillary column bonded with 5% phenylmethyl silicone as stationary phase.The results showed that the linear correlation coefficients of propiconazole and prochloraz were of 0.999 9 and 0.999 8, respectively; the standard deviations were of 0.035 and 0.028; the variation coefficients were of 0.33% and 0.13%; and the average recoveries were of 99.88% and 99.95%, respectively.
Key words:propiconazole; prochloraz; GC
作者简介:潘光飞(1979-),男,浙江温州人,主要从事农药检测与研究(E-mail:609179300@qq.com)
收稿日期:2019-10-13