第 51 卷第 1 期Vol. 51 No. 1
2021 年 2 月Feb 2021

所属栏目:有机合成原料

苯氧乙醇的纯化工艺研究
寇 然,金一丰,周 扬,黄鑫荣,刘 凯 (浙江皇马科技股份有限公司,浙江 上虞 312369)
摘 要:以工业级苯氧乙醇粗品为原料,通过减压精馏和大孔吸附剂吸附两步纯化工艺得到主含量纯度高(≥99.9%,GC),苯酚含量低(≤5 mg·kg-1,LC)的化妆品用原料苯氧乙醇,两步收率90%,该制备工艺路线简单,生产成本低,适合工业化生产。
关键词:苯氧乙醇;大孔吸附剂;减压精馏
中图分类号:TQ243.4  文献标识码:A  文章编号:1009-9212(2021)01-0040-05
Purification of Phenoxyethanol for Cosmetics
KOU Ran, JIN Yi-feng, ZHOU Yang, HUANG Xing-rong, LIU Kai (Zhejiang Huangma Technology Co.,Ltd., Shangyu 312369, China)
Abstract:Using crude phenoxyethanol as the raw material, through a two-step purification process including vacuum rectification and macroporous adsorbent adsorption, the phenoxyethanol for cosmetics a purity of 99.9% and limited phenol of 5 mg·kg-1 was obtained. This preparation process has many advantages including simple operation, low in cost, and suitable for industrial production.
Key words:phenoxyethanol; macroporous adsorbent; rectification
作者简介:寇 然(1992—),男,安徽滁州人,博士,主要从事表面活性剂及中间体的合成研究及工业化生产(E-mail:2559553600@qq.com)
收稿日期:2020-12-25