第 33 卷第 3 期Vol. 33 No. 3
2003 年 6 月Jun 2003

所属栏目:其它

2-氯丙酰基苯胺的合成
陈华; 沈菊李; 项菊萍; 周海安; 武宏科; 史鸿鑫(浙江工业大学化工学院; 浙江杭州; 310014)
摘 要:采用丙酸、氯气和苯胺,在催化剂作用下两步合成了除草剂萘丙胺中间体2-氯丙酰基苯胺,并以正交试验法优化了工艺条件,合成总收率达到80%。
关键词:萘丙胺; 2-氯丙酰基苯胺; 氯化
中图分类号:O623.64  文献标识码:A  文章编号:1009-9212(2003)03-0021-02
Synthesis of 2-chloropropionanilide
CHEN Hua etc.(Institute of Chemical Engineering; Zhejiang University of Technology; Zhejiang Hangzhou; 310014; China)
Abstract:Chloropropionanilide and intermediates of naproanilide were synthesized from propionic acid, chlorine, and aniline in the presence of catalysts through two steps. The reaction conditions were optimized. The total yield of two steps is 80%.
Key words:chloropropionanilide; naproanilide; chlorization
收稿日期:2002-12-09
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