| 第 33 卷第 3 期 |  | Vol. 33 No. 3 | | 2003 年 6 月 | Jun 2003 |
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所属栏目：其它
杂多酸(盐)催化新型香料草莓酯的合成 |
| 刘杰凤; 农兰平; 蒋维(茂名学院; 广东茂名; 525000) |
| 摘 要：采用硅钨酸铝作催化剂 ,以乙酰乙酸乙酯和 1 ,2 丙二醇为原料合成草莓酯。优化的反应条件为 :0 2mol乙酰乙酸乙酯 ,0 2mol1 ,2 丙二醇 ,40ml环己烷 ,0 3 g硅钨酸铝 ,反应 3 5h ,草莓酯收率达 81 6%。产物经理化检验和红外光谱确证 |
| 关键词：草莓酯; 杂多酸; 合成 |
| 中图分类号：TQ655 文献标识码：A 文章编号：1009-9212(2003)03-0019-02 |
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| Synthesis of a New Type Perfume fraistone Catalyzed by Heteropoly Acids(salt) |
| LIU Jie feng etc.（Maoming college; Guangdong maoming 525000; China） |
| Abstract：Fraistone was synthesized with reaction of Ehyl Acetyl acetate and 1,2 Propanediol, by aluminnm silicolungstie as catatlyst. The optimum conditions are follows: the ratio of ethyl acetate, 1,2 Propanediol, Cyclohexane,Aluminnm Silicolungstie is 0.2?mol:0.2?mol:40?ml:0.3?g, reaction for 3.5 hours.The yield reaches 81.6%. The product was characterized by the physical and chemical character, and spectra. |
| Key words：fraistone; heteropoly acids; synthesis |
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收稿日期：2003-04-03
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