| 第 34 卷第 2 期 |  | Vol. 34 No. 2 | | 2004 年 4 月 | Apr 2004 |
|
所属栏目：分析与测试
高效液相色谱法同时测定吡虫啉和多效唑 |
| 王安群; 彭凤仙; 邓益群(长沙环境保护技术学院监测系; 湖南长沙) |
| 摘 要：采用高效液相色谱法连续测定吡虫啉和多效唑的含量,该方法中吡虫啉和多效唑标准偏差分别为0.94和0.59,变异系数为0.58%和0.45%,在0 8～15 0mg/L和1 5～25mg/L的范围内与峰高呈良好的线性关系,回收率为99 6%和98 9%,其相关线性系数为0 9995和0 9989,满足在水样、秧苗、稻谷样品中的检测要求,方法简便、快速、准确。 |
| 关键词：吡虫啉; 多效唑; 高效液相色谱法; 连续测定 |
| 中图分类号：657.7+2 文献标识码：A 文章编号：1009-9212(2004)02-0072-02 |
|
| A Method for Continuous Determinatio of Imidacloprid and Paclobutrazol by High Performance Liquid Chromatography |
| WANG An-qun; PENF Feng-xian; DENG Yi-qun （Changsha Environment Protection Ocational College; Changsha 410004; China） |
| Abstract：A method for continuous determination of imidacloprid and paclobutrazol is described by high performance liquid chromatography. A baseline resolution of imidacloprid and paclobutrazol with impurities was achieved on Bondapak C_(18) column within 12 min by using methanol-water system (70∶30 by voiume) as a mobile phase at flow rate of 1ml/min, and the eluate was monitored at λ=254nm. Imidacloprid and paclobutrazol in the liner range of 0.8～15.0mg/L and 1.5～25mg/L has a good linearity with its high (r=0.9995 ... |
| Key words：imidacloprid; paclobutrazol; high performance liquid chromatography; continuous determination |
|
收稿日期：2003-11-13
|
| 阅读全文 |
|