第 31 卷第 2 期 | | Vol. 31 No. 2 | 2001 年 4 月 | Apr 2001 |
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所属栏目:其它
改性环糊精手性毛细管柱的研制及拆分机理 |
阎建辉; 唐阔文;(岳阳师范学院化学化工系;) |
摘 要:合成了四种改性 β 环糊精手性固定相 ,对几类手性化合物和芳香异构体进行了拆分 ,并研究了其可能的拆分机理 ,同时对毛细管柱的色谱性能进行了考察。 |
关键词:改性环糊精; 手性固定相; 毛细管气相色谱; 拆分机理; |
中图分类号:O657.8 文献标识码:A 文章编号:1009-9212(2001)02-0013-03 |
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Preparation of Derivatized Cyclodextrins Capillary columns and Investigation on Separation Mechanism |
YAN Jian hui; TANG Kuo wen (College Chemical Engineering; Yueyang Normal University; Hunan Yueyang 414000; China); |
Abstract:Four derivatized cyclodextrins have been synthesized and coated in fused silica capillary columns as stationary phases. A series of enantiomers have been separated on the four stationary phases. The separation mechanism of them has been studied, and the chromatography performance has been investigated. |
Key words:derivatized cyclodextrins; chiral stationary phases; capillary gas chromatography; separation mechanism; |
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收稿日期:2000-12-25
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