第 36 卷第 3 期 |  | Vol. 36 No. 3 | 2006 年 6 月 | Jun 2006 |
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所属栏目:分析与测试
三唑嘧啶酮原药的高效液相色谱分析 |
胡礼; 黄超群; 熊莉莉(湖南化工研究院; 湖南长沙) |
摘 要:采用高效液相色谱法,使用C18(ODS)分离柱、甲醇∶水为流动相和二极管阵列检测器,用外标法测定三唑嘧啶酮原药中有效成分的含量。方法的标准偏差为0.22%,变异系数为0.23%,线性相关系数为0.999 7,回收率为98.49%~100.5%。 |
关键词:三唑嘧啶酮; 高效液相色谱; 分析 |
中图分类号:TQ457.2+7 文献标识码:A 文章编号:1009-9212(2006)03-0062-02 |
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Analysis of PP796(Emetic)by HPLC |
HU Li; HUANG Chao-qun; XIONG Li-li(Hunan Research Institute of Chemical Industry; Changsha 410007; China) |
Abstract:A quantitative analysis method of the PP796(emetic)was developed by HPLC with ODS column and methanol: water as mobile phase.Results showed that the standard deviation was 0.22%,the coefficient of variation was 0.23%,the linear correlation coefficient was 0.999 7,and recovery was 98.49%~100.5%. |
Key words:PP796(emetic); HPLC; analysis |
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收稿日期:2005-12-20
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