第 37 卷第 5 期 | | Vol. 37 No. 5 | 2007 年 10 月 | Oct 2007 |
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所属栏目:医药及中间体
大孔树脂提取纯化姜黄素的研究 |
黄灵芝,李丽峰,董君英
(长沙理工大学 化学与环境工程学院,湖南 长沙 410077) |
摘 要:通过考察不同大孔树脂对姜黄素吸附与解吸性能,探讨大孔树脂对姜黄素的吸附和解吸工艺,筛选出适用的大孔树脂型号。实验结果表明S-8大孔树脂对姜黄素吸附能力较大,并且解吸性能好,吸附阶段的泄漏点为1.0,饱和点为8.9,解吸阶段的适用乙醇浓度为100%,因此,适合作为分离纯化姜黄素的树脂型号。 |
关键词:姜黄素;吸附;解吸;大孔树脂 |
中图分类号:R914.5 文献标识码:A 文章编号:1009-9212(2007)05- 0024-03 |
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Separation and Purification of Curcumin with Macroporous Resins |
HUANG Ling-zhi LI Li-feng DONG Jun-ying
(College of Chemistry & Environmental Engineering,Changsha University of Science & Technology,Changsha 410077,China) |
Abstract:The suitable macroporous resin was selected through investigation of the absorption and elution of various macroporous resins for curcumin and their oplimum technological parameter. The experimental results show that S-8 macroporous resin is suitable for separation and purification of curcumin because of its excellent adosorption capacities and elution ability. In the adsorption phase,when the ratio between curcumin and S-8 macroporous resin is 1.0,curcumin appeared leaking,There was no adsorptiom of curcumin on the resin when the ratio was 8.9. In the elution phase,the optimum alcohol concentration is 100%. |
Key words:curcumin;adsorption;elution;macroporous resins |
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作者简介:黄灵芝(1972-),女,湖南湘潭人,讲师,硕士,从事分析化学的研究。(E-mail:hlz-121@163.com)
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收稿日期:2007-08-27
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